Description
Specifications Table
Product Name – Methyltitanium(IV) triisopropoxide, 1M solution in THF, AcroSeal®
Quantity/Pack Size – 100ML
Form – Liquid (Solution)
Grade – AcroSeal® (Moisture-Sensitive)
Application – Catalysis, organic synthesis, thin-film deposition
Product Overview
Methyltitanium(IV) triisopropoxide is a highly reactive organometallic compound supplied as a 1M solution in tetrahydrofuran (THF) under the AcroSeal® brand, ensuring maximum protection against moisture and oxidation. This reagent is widely utilized in advanced organic synthesis, particularly in cross-coupling reactions, polymerization processes, and the formation of titanium-based thin films. The THF solvent enhances solubility and reactivity, making it ideal for precise stoichiometric applications. The AcroSeal® packaging guarantees long-term stability by preventing exposure to atmospheric moisture, which can degrade the compound. Each batch undergoes rigorous quality control to ensure consistent purity and concentration, minimizing variability in experimental outcomes. The solution’s high reactivity necessitates careful handling under inert conditions, typically in a glove box or with Schlenk techniques. Its compatibility with a range of organic substrates makes it a versatile tool for synthesizing complex molecular architectures, including pharmaceutical intermediates and specialty materials. Researchers benefit from its predictable behavior in controlled environments, enabling reproducible results in demanding applications.
FAQs
1. What is the shelf life of Methyltitanium(IV) triisopropoxide in THF when stored properly?
The solution remains stable for up to 12 months from the date of manufacture when stored unopened in its original AcroSeal® packaging at temperatures between 2°C and 8°C. Avoid exposure to air or moisture.
2. Is this reagent compatible with glassware, or are specific materials recommended?
While compatible with standard borosilicate glass, prolonged contact may etch the surface due to the reagent’s reactivity. For long-term storage or reactions, use PTFE-lined or stainless-steel containers to prevent contamination.
3. Can this solution be diluted further, and if so, what solvents are suitable?
Dilution is possible using anhydrous solvents like hexane, toluene, or additional THF. Ensure all solvents are moisture-free and handled under inert gas to maintain the reagent’s integrity.
4. What safety precautions are essential when handling this compound?
Due to its pyrophoric nature, handle only in a well-ventilated fume hood or glove box. Use flame-resistant lab wear, safety goggles, and nitrogen-purged equipment to prevent ignition or decomposition.
5. Are there alternatives to THF as a solvent for this reagent?
Alternatives like diethyl ether or dichloromethane can be used, but THF is preferred for its balance of solubility and stability. Solvent choice may affect reaction rates and should be validated for specific applications.
